Nuclear Magnetic Resonance (NMR): Theory, Applications and Technology

Doddapuneni Krishna Rao, PhD (Editor)
Magnetic Resonance Spectroscopy & Metabolic Imaging Group, Biomedical Science Institutes (A*-STAR), Singapore

Series: Physics Research and Technology
BISAC: SCI078000




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This book is mainly focused on basic concepts and different applications of NMR from the small molecules to biological macromolecules. This book was made with contributions from different authors all over the world who are working on different aspects of science with the common tool of NMR. Different types of NMR methods used to analyze the structures of small molecules and proteins and the complete story of how one can solve the structure of the new drug molecule are explained.

A review on NMR structural and dynamical aspects of the death domain super family proteins, and the metabolic profile and quantification of metabolites in PGI cherry tomatoes using solid state NMR are explained. Also, the usefulness of Proton Nuclear Magnetic Resonance (1H NMR) spectroscopy in the study of edible oils and fats, and of food lipids in general, from both qualitative and quantitative points of view is mentioned. (Imprint: Nova)



Chapter 1 - The Role of NMR in Structural Elucidation of Small Molecules and Proteins (pp. 1-26)
Nadeem Khan and Doddapuneni Krishna Rao (Jai Research Foundation, Gujrat, India and others)

Chapter 2 - Structural Characterization of Fluconazole Drug Using NMR Spectroscopy (pp. 27-42)
Sachin Kumar and Doddapuneni Krishna Rao (Jubilant Chemsys Ltd. R and D Centre Noida, Noida, Uttar Pradesh, India and others)

Chapter 3 - Off-Pathway Intermediate(s) in the Refolding of Alkaline Ferrocytochrome c: A Pulse-Labeling HX NMR Study (pp. 43-60)
Doddapuneni Krishna Rao, N. Prakash Prabhu and Abani K. Bhuyan (Singapore BioImaging Consertum, A*STAR, Singapore and others)

Chapter 4 - Aromatic Ring-Flip Motions in Proteins by EXSY NMR (pp. 61-82)
Doddapuneni Krishna Rao and Abani K. Bhuyan (Singapore BioImaging Consertum, A*STAR, Singapore and others)

Chapter 5 - NMR Spectroscopic Characterization of Death Domain Superfamily Proteins: Structures, Dynamics and Interactions (pp. 83-110)
Yufeng Wei and Edward C. Twomey (Institute of NeuroImmune Pharmacology, Seton Hall University, South Orange, NJ, USA and others)

Chapter 6 - Theories and Applications in Solid-State Nuclear Magnetic Resonance Spectroscopy (pp. 111-162)
Eugene Stephane Mananga, Betina Suzanne Mananga and Alicia Errolene Reid (Harvard University, Harvard Medical School, and Massachusetts General Hospital, Center for Advanced Medical Imaging Sciences, Division of Nuclear Medicine and Molecular Imaging Physics, Department of Radiology, Boston, Massachusetts, USA and others)

Chapter 7 - A Quantitative 1H HR-MAS Study of the Metabolic Profile of the PGI Cherry Tomato of Pachino (pp. 163-178)
Carmelo Corsaro, Domenico Mallamace and Giacomo Dugo (Dipartimento di Fisica e Scienze della Terra, Università di Messina, Messina, Italy and others)

Chapter 8 - A and B Occupation Rates of Mixed A2-xBxZnCl4 (A = NH4, Rb, Cs; B = Rb, Cs; x = 0, 1, and 2) Single Crystals by Nuclear Magnetic Resonance (pp. 179-220)
Ae Ran Lim (Departments of Science Education and Carbon Fusion Engineering, Jeonju University, Jeonju, Korea)

Chapter 9 - 1H NMR, a Tool for Qualitative and Quantitative Study of Food Lipid Composition and of Its Evolution in Degradation Processes (pp. 221-250)
Andrea Martínez-Yusta, Encarnación Goicoechea and Maria D. Guillén (Food Technology, Lascaray Research Center, Faculty of Pharmacy, University of the Basque Country (UPV/EHU)


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